Iranian Journal of Materials Science and Engineering
Iran University of Science & Technology
Thu, Nov 14, 2024
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Volume 11, Issue 3 (september 2014)
IJMSE 2014, 11(3): 24-31 |
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Azizi, Soltanieh. STUDY ON NIOBIUM CARBIDE COATING FORMATION ON AISI L2 STEEL USING THERMO-REACTIVE DEPOSITION METHOD. IJMSE 2014; 11 (3) :24-31
URL: http://ijmse.iust.ac.ir/article-1-679-en.html
URL: http://ijmse.iust.ac.ir/article-1-679-en.html
Abstract: (19608 Views)
In the present research, to form niobium carbide coating on the surface of AISI L2 steel Thermo-Reactive
Deposition method (TRD) in a molten bath was used. Niobium carbide coating treatment was carried out at 1173 K,
1273 K, and 1373 K for 2, 4, and 8 hours. The molten bath contained 20wt.% borax (Na2B4O7), 5 wt.% boric acid
(B2O3), and 75 wt.% ferro-niobium. The presence and properties of the coated layer were studied by means of Optical
Microscopy (OM), Scanning Electron Microscopy (SEM), and X-Ray Diffraction (XRD) analysis. The thickness of
coating ranged between 6.6 µm to 33µm depending on treatment time, and temperature. The effects of treatment time
and temperature on the coating thickness were studied. Kinetic study of the formation of NbC coating showed that
growth of the coating is under the control of diffusion. The activation energy of the process was estimated to be 122
kJ/mol. A practical formula to estimate the coating thickness was suggested.
Type of Study: Research Paper |
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