Showing 5 results for Microstructure.
Javadpour J., Sakhaii K., Masihiyanpour A.a.,
Volume 1, Issue 4 (12-2004)
Abstract
Thin sheets of hydroxyapatite were fabricated by tape casting process. The non-aqueoustape casting formulation was optimized by adjusting the concentration of organic additivesspecially those of binder and plasticizer in the slurry. The optimized slurry was cast on a glasscarrier using a designed laboratory scale doctor blade. Following a binder removal stage, thetapes were sintered at different temperatures in air atmosphere. Heat treatment at 1250 °C led tothe formation of a dense microstructure as was evidenced by the scanning electron microscopy.
A. Mohassel, A. H. Kokabi, P. Davami,
Volume 8, Issue 4 (12-2011)
Abstract
The wide-gap aluminothermic rail welds with root opening of 50-70 mm were produced using plain carbon steel rail and non-alloy aluminothermic charge. Mechanical properties and micro-structure of the weld metal and HAZ as well as the impact energy and the fracture toughness of the welds were investigated. The yield and tensile strength of wide-gap welds were about 98% and 95% of the base metal, respectively. Both minimum and maximum hardnesses of the joint were seen in HAZ which were related to the grain coarsening and normalizing, respectively. The mean value of wide-gap weld fracture toughness is more than narrow-gap weld. Moreover, trans-granular cleavage indicated the brittle fracture mode of the weld metal.
M. J. Tafreshi, B. Dibaie, M. Fazli,
Volume 9, Issue 1 (3-2012)
Abstract
Abstract: A thermodynamic model was used to find out the optimum temperature for the growth of ZnS single crystals in closed ampoules by chemical vapor transport technique. Based on this model 1002 °C was found to be optimum temperature for 2 mg/cm3 concentration of transporting agent (iodine). ZnS Crystals were grown in optimum (1002 °C) and non-optimum (902 °C and 1102 °C) temperatures. The composition structure and microstructure of the grown crystals were studied by Atomic absorption spectroscopy, X-ray diffraction and Scanning electron microscopy measurements. Properties of the grown crystals were correlated to the growth conditions especially a stability in mass transport along the closed tube length.
A. Najafi, F. Golestani-Fard, H. R. Rezaie,
Volume 11, Issue 1 (3-2014)
Abstract
Mono dispersed nano SiC particles with spherical morphology were synthesized in this project by hydrolysis and condensation mechanism during sol gel processing. pH, temperature and precursor’s ratio considered as the main parameters which could influence particles size. According to DLS test results, the smallest size of particles in the sol (<5nm) was obtained at pH<4. It can be observed from rheology test results optimum temperature for achieving nanometeric gel is about 60 ˚C. The optimum pH values for sol stabilization was (2-5) determined by zeta potentiometery. Si 29NMR analysis was used in order to get more details on final structure of gel powders resulted from initial sol. X-ray diffraction studies showed sythesized powder consists of β-SiC phase. Scanning electron microscopy indicated agglomerates size in β-SiC synthesis is less than 100 nm. Finally, TEM studies revealed morphology of β-SiC particles treated in 1500˚C and after 1hr aging is spherical with (20-30) nm size
M. Demouche, E. H. Ouakdi, R. Louahdi,
Volume 16, Issue 3 (9-2019)
Abstract
In this study, high-carbon, chromium alloy steel (100Cr6) having the initial spheroidized microstructure was welded using the rotary friction welding method. The effects of process parameters such as friction time and friction force were experimentally investigated. The friction welded joints were produced of two 100Cr6 steel rods. In order to examine the microstructure and mechanical properties of the friction welded 100cr6 steel joints, tensile and hardness tests were conducted. The microstructure of weld zone was examined by optical microscopy. It was found that after cooling, martensitic structure is obtained at the core and periphery of the weld joint. It was found that the tensile strength of friction welded samples is increased with increasing time and force of friction up to a certain level and then decreases again. Hardness measurements show a higher hardness at the centre of the weld joint in comparison with its periphery.
