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HYDROTHERMAL SYNTHESIS OF YTTRIUM ORTHOVANADATE (YVO4) AND ITS APPLICATION IN PHOTO CATALYTIC DEGRADATION OFSEWAGE WATER
P. Karimi, K. S. Hui, K. Komal,
Volume 7, Issue 3 (8-2010)
Abstract

Abstract:

(Y2O3) and ethyl acetate as a mineralizer by hydrothermal method at a low temperature (T=.230°C, and

P=100bars).The as-prepared powders were characterized by X-ray Diffraction (XRD), Fourier Transform Infrared

Spectroscopy (FTIR), Scanning Electron Microscopy (SEM), UV-V Spectroscopy and Chemical Oxygen Demand

(COD) of the sewage water, respectively. The results show that hydrothermal method can greatly promote the

crystallization and growth of YVO4 phase. XRD pattern clearly indicates the tetragonal structure and crystallanity. An

FTIR spectrum of the YVO4 shows the presence of Y-O and V-O bond, respectively. The presence of these two peaks

indicates that yttrum vanadate has been formed. UV-V is absorption spectra suggesting that YVO4 particles have

stronger UV absorption than natural sunlight and subsequent photocatalytic degradation data also confirmed their

higher photocatalytic activity.

In this paper, YVO4 powder was successfully synthesized from Vanadium Pentaoxide (V2O5), Yttrium Oxide
High Photocatalytic Performance in the Photodegradation of MB Dye of Photocatalytic Efficiency of ZnO/Fe3O4 and TiO2/Fe3O4 Under Visible Light Irradiation
M.j Kadhim, Fatima Allawi, M. A. Mahdi, Sami Najah Abaas,
Volume 19, Issue 3 (9-2022)
Abstract
     Zinc Oxide (ZnO) nanorods and titanium dioxide (TiO2) nanostructures thin films were prepared onto glass substrates by the chemical bath deposition (CBD) method. The ZnO was structured as nanorods (NRs) while TiO2 was formed as nanoflowers plate as confirmed by Field-Emission Scanning Electron Microscope (FESEM) images. The ZnO/Fe3O4 and TiO2/Fe3O4 nanostructures thin films were prepared via drop-casting Fe3O4 NPs onto the grown ZnO and TiO2 nanostructures thin films. The diameter of Fe3O4 NPs was deposited onto ZnO NRs thin films and TiO2 nanostructures thin films was ranged from 8nm to 59nm with dominated range between 10nm to 30 nm.  The crystalline structure of prepared samples was investigated through X-ray diffraction (XRD) method. However, the particles size of Fe3O4  was estimated  by XRD as well as FESEM images was around 22 nm. The photocatalytic activity of the as-prepared ZnO/Fe3O4 and TiO2/Fe3O4 nanostructures thin films was investigated against methylene blue (MB) dye at room temperature with a pH value of 10 under different exposure time by visible light. The photodegradation rate of MB dye by ZnO/Fe3O4 and TiO2/Fe3O4 nanostructures thin films was higher than that obtained by ZnO and TiO2 nanostructures thin films. The best photodegradation rate of MB dye was 100% after exposure time of 180 min was obtained by ZnO/Fe3O4 nanostructures thin film whereas it was 82% for TiO2/Fe3O4 nanostructures thin films after exposure time of  240 min.  
 
Property Analysis of β-Tetragonal Bismite Thin Films: Varied Concentrations and Enhanced Photocatalytic Efficiency
Hella Houda, Guettaf Temam Elhachmi, Hachemi Ben Temam, Saâd Rahmane, Mohammed Althamthami,
Volume 21, Issue 0 (3-2024)
Abstract
In this study, we thoroughly examine β-Bi2O3 thin films as potential photocatalysts. We produced these films using an environmentally friendly Sol Gel method that is also cost-effective. Our research focuses on how different precursor concentrations, ranging from 0.1 M to 0.4 M, affect the photocatalytic performance of these films. We conducted a comprehensive set of tests to analyze various aspects of the films, including their structure, morphology, topography, optical properties, wettability, and photocatalytic capabilities. These tests provided us with a well-rounded understanding of the films' characteristics. To assess their photocatalytic efficiency, we used Methylene Blue (MB) as a contaminant and found that the films, particularly those with a 0.1 M concentration, achieved an impressive 99.9% degradation of MB within four hours. The 0.1 M film had a crystalline size of 39.7 nm, an indirect band gap of 2.99 eV, and a contact angle of 51.37°. Our findings suggest that β-Bi2O3 films, especially the 0.1 M variant, have promising potential for treating effluents from complex industrial dye processes. This research marks a significant step in utilizing sustainable materials to address pollution and environmental remediation challenges.
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